This reference details particle characterization, dynamics, manufacturing, handling, and processing for the employment of multiphase reactors, as well as procedures in reactor scale-up and design for applications in the chemical, mineral, petroleum, power, cement and pharmaceuticals industries. The authors discuss flow through fixed beds, elutriation and entrainment, gas distributor and plenum design in fluidized beds, effect of internal tubes and baffles, general approaches to reactor design, applications for gasifiers and combustors, dilute phase pneumatic conveying, and applications for chemical production and processing. This is a valuable guide for chemists and engineers to use in their day-to-day work.

This book discusses the diverse array of particles that are found in coatings from both a physical and a performance standpoint. It also describes the fundamentals of particle behavior and shows how these affect the performance and properties of their end-use applications. It consists of nineteen chapters, demonstrating the wide range of types of particles found in coatings as well as the diversity of the important attributes they hold. The authors also present a forward looking view of current issues and trends in the coatings industry. In addition, a chapter on the use of particles in paper laminate, a closely aligned field, is included. This book is of interest to formulators of any type of coatings as well as researchers in aligned fields that use high volumes of small particles, such as the plastics and paper industries.

This book presents part of the proceedings of the Manufacturing and Materials track of the iM3F 2021 conference held in Malaysia. This collection of articles deliberates on the key challenges and trends related to manufacturing as well as materials engineering and technology in setting the stage for the world in embracing the Fourth Industrial Revolution. It presents recent findings with regard to manufacturing and materials that are pertinent toward the realizations and ultimately the embodiment of Industry 4.0, with contributions from both industry and academia.

Chemical Product Design: Towards a Perspective through Case Studies provides a framework for chemical product design problems which are clearly defined together with different solution approaches. This book covers the latest methods and tools currently available in the field and discusses future challenges that the chemical industry is faced with. It focuses on important issues of chemical product design and provides a good overview on industrial chemical product design problems through case studies supplied by leading experts. The editors of Chemical Product Design teach chemical product design at graduate level courses and also serve as consultants for various chemical companies. They have also developed experimental techniques for chemical product design as well as computer-aided design methods and tools.
* highlights important issues of chemical product design through case studies
* case studies supplied by leading experts in chemical product design
* provides a complete framework for chemical product design

Volumes 21 and 22 of Advances in Chemical Engineering contain ten prototypical paradigms which integrate ideas and methodologies from artificial intelligence with those from operations research, estimation andcontrol theory, and statistics. Each paradigm has been constructed around an engineering problem, e.g. product design, process design, process operations monitoring, planning, scheduling, or control. Along with the engineering problem, each paradigm advances a specific methodological theme from AI, such as: modeling languages; automation in design; symbolic and quantitative reasoning; inductive and deductive reasoning; searching spaces of discrete solutions; non-monotonic reasoning; analogical learning;empirical learning through neural networks; reasoning in time; and logic in numerical computing. Together the ten paradigms of the two volumes indicate how computers can expand the scope, type, and amount of knowledge that can be articulated and used in solving a broad range of engineering problems.
Key Features
* Sets the foundations for the development of computer-aided tools for solving a number of distinct engineering problems
* Exposes the reader to a variety of AI techniques in automatic modeling, searching, reasoning, and learning
* The product of ten-years experience in integrating AI into process engineering
* Offers expanded and realistic formulations of real-world problems

Reviews actual events and case studies that chronicle the evolution of safety precautions, the establishment of emergency planning requirements, and the design of advanced warning and control systems This authoritative reference/text analyzes health and hazard risk assessment in commercial, industrial, and refining industries-emphasizing legal requirements, emergency planning and response, safety equipment, process implementation, and occupational and environmental protection exposure guidelines. Presents applications and calculations for risk analysis of real systems, as well as numerous end-of-chapter examples and references Containing practical process diagrams for plant equipment, valves, piping, and control systems, Health, Safety, and Accident Management in the Chemical Process Industries covers laws for disaster planning by federal, state, and local governments the implementation of safeguards in chemical process design proper plant operation when using reactors, mass transfer units, heat exchangers, and ancillary devices the physical and chemical properties and health effects of chlorine, ammonia, hydrogen fluoride, sulfuric acid, and ethylene dose-response evaluation and risk characterization and more Offering system checklists as well as effective evacuation procedures, Health, Safety, and Accident Management in the Chemical Process Industries is an invaluable resource for chemical, industrial, manufacturing, and environmental engineers; public safety, human services, and health care managers and administrators; social workers; and public policy specialists; and an ideal text for upper-level undergraduate and graduate students in these disciplines.

This book introduces in a non-traditional way the laws of physical chemistry and its history starting in the 16th century. It reveals to the reader how physical chemists try to understand chemical processes in terms of physical laws. Hydrogen is the main focus of the book as its simplicity makes the relevant laws of nature easy to explain and its role in energetics in the near future is clear. With the basics at hand, the importance of hydrogen as a raw material in the industry and as an energy carrier in the near future is made clear. Only simple chemical processes are discussed and very little mathematics is used. Both the pleasure and use of this field of research are revealed to the interested reader. The expected readership is made of high school students, non-chemistry major freshmen, and general audience with an interest in chemistry. The real aim of this book is to prompt the reader to wonder.

This handbook seeks to facilitate the selection, design and operation of large-scale industrial crystallizers that process crystals with the proper size distribution, shape and purity sought - including cooling, evaporation, drowning-out reaction, melt, and related crystallization techniques. This new edition offers new results on direct-contact cooling crystallization. It lists the properties of over 170 organic and inorganic crystallization systems.

Corinna Reisinger has developed a new organocatalytic asymmetric epoxidation of cyclic and acyclic , -unsaturated ketones. In this thesis, Corinna documents her methodology, using primary amine salts as catalysts, and hydrogen peroxide as an inexpensive and environmentally benign oxidant. She describes the unprecedented and powerful catalytic asymmetric hydro peroxi dation of , -enones, a process which produces optically active five-membered cyclic peroxyhemiketals in a single operation. She also proves the versatility and synthetic value of the cyclic peroxyhemiketals by converting them into highly enantioenriched acyclic and cyclic aldol products. Currently, these cyclic aldol products are inaccessible by any other synthetic means. Furthermore, cyclic peroxyhemiketals are precursors to optically active 1,2-dioxolanes which are of biological relevance. This work is a breakthrough in the field of asymmetric epoxidation chemistry and outlines the most efficient method in the literature for generating highly enantioselective cyclic epoxyketones known to date.

This book systematically covers the fundamentals and applications of modified biochar. The 19 chapters are divided into 3 sections that provide a holistic overview for researchers from all related fields. Section 1 and 2 present the pyrolysis process, including the advantages and limitations of the physical, chemical, and biological modification methods and characterization of modified biochar. Section 3 highlights the wide spectrum of applications of modified biochar in fuel cells and batteries, remediation of organic and inorganic contaminants from soil and water and soil fertilization. Given its scope, the book appeals to a broad readership in various fields of chemical engineering, materials science, and environmental science.

This book presents part of the proceedings of the Manufacturing and Materials track of the iM3F 2020 conference held in Malaysia. This collection of articles deliberates on the key challenges and trends related to manufacturing as well as materials engineering and technology in setting the stage for the world in embracing the fourth industrial revolution. It presents recent findings with regards to manufacturing and materials that are pertinent towards the realizations and ultimately the embodiment of Industry 4.0, with contributions from both industry and academia.

This new volume introduces the applications of microfluidic systems to facilitate biotechnological and biomedical processes. It provides an overview on cutting-edge technologies, summarizes traditional and modern fabrication methods and highlights recent advances regarding the application of lab-on-a-chip (LoC) systems for bioanalytical purposes. This book is ideal for research scientists and students interested at the cross-section between biotechnology, chemistry and chemical engineering.

Siting of permanent and temporary buildings in process areas requires careful consideration of potential effects of explosions and fires arising from accidental release of flammable materials. This book, which updates the 1996 edition, provides a single-source reference that explains the American Petroleum Institute (API) permanent (752) and temporary (753) building recommended practices and details how to implement them. New coverage on toxicity and updated standards are also highlighted. Practical and easy-to-use, this reliable guide is a must-have for implementing safe building practices.

The second edition of this popular industrial guide describes over 2,800 currently available epoxy resins, curing agents, compounds, and modifiers, based on information supplied by 71 manufacturers or distributors of these products. Epoxy resins have experienced tremendous growth since their introduction in the 1950s. Future growth will be in new markets in the specialty performance areas and high-technology applications. Each raw material or product is described, as available, with typical assay or checkpoint figures and a brief summary of important features or applications. Additional sections useful to the reader are the Suppliers' Addresses and a Trade Name Index.

Volumes 21 and 22 of Advances in Chemical Engineering contain ten prototypical paradigms which integrate ideas and methodologies from artificial intelligence with those from operations research, estimation andcontrol theory, and statistics. Each paradigm has been constructed around an engineering problem, e.g. product design, process design, process operations monitoring, planning, scheduling, or control. Along with the engineering problem, each paradigm advances a specific methodological theme from AI, such as: modeling languages; automation in design; symbolic and quantitative reasoning; inductive and deductive reasoning; searching spaces of discrete solutions; non-monotonic reasoning; analogical learning;empirical learning through neural networks; reasoning in time; and logic in numerical computing. Together the ten paradigms of the two volumes indicate how computers can expand the scope, type, and amount of knowledge that can be articulated and used in solving a broad range of engineering problems.
Key Features
* Sets the foundations for the development of computer-aided tools for solving a number of distinct engineering problems
* Exposes the reader to a variety of AI techniques in automatic modeling, searching, reasoning, and learning
* The product of ten-years experience in integrating AI into process engineering
* Offers expanded and realistic formulations of real-world problems

This volume is concerned with the use of over 16 million tonnes of oils and fats by the oleochemical industry worldwide. It provides an overview of oleochemicals at research and professional level, with an emphasis on their industrial production and applications. Approximately half of the chapters consider matters of relevance throughout the oleochemical industry, while the remainder deal with applications. Authors are drawn from industrial and academic laboratories around the world.

The book is directed at chemists and technologists working on the production and use of oleochemicals, analytical chemists and quality assurance personnel, and lipid chemists in academic research laboratories.

This book is a comprehensive introduction on infrared anti-transparent materials and their applications in anti-reflective and protective coatings. Optical, mechanical and thermal properties and preparations of various kinds of films, such as amorphous diamond films, germanium carbide films, boron phosphide films, alumina films and yttrium oxide film are discussed in detail making it suitable for material scientists and industrial engineers.

Facilitates the selection of appropriate procedures when using SPE to clean up samples, extract, and concentrate analytes or eliminate interferring substances in sample analyses. This comprehensive reference/text demonstrates the relationship of the basic theory of solid-phase extraction (SPE) to chromatography-illustrating how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques, including gas chromatography, mass spectrometry, and high-performance liquid chromatographic analyses. Provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening Written by world-renowned experts in the field, Solid-Phase Extraction thoroughly covers digital chromatography, the basic elements of SPE, capacity and selectivity, and the mechanisms of adsorption and desorption nonpolar, polar, and ion-exchange extraction mechanisms, as well as complexation, chelation, and covalent retention actual vs. ideal performance and predictive SPE, as well as expert systems using and eliminating secondary interactions and mixed-mode SPE preparing and handling biological fluids, particulates, solid and air samples by SPE, including problem components in a sample matrix creating affinity sorbents and the properties and uses of affinity SPE automation approaches, techniques for automated method development, off-line solid extraction, and on-line SPE complementary use of SPE and supercritical fluid extraction and more Containing helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more, Solid-Phase Extraction is an essential, on-the-job reference for analytical, environmental, synthetic organic, and medicinal chemists and biochemists; and toxicologists; and an ideal textbook for upper-level undergradua

This text aims to offer the best of ion exchange science conducted in the countries of the former Soviet Union. It reviews the multidisciplinary study at the nexus of physical, organic, inorganic and biological chemistries, and progresses from theoretical fundamentals to practical applications in manufacturing, mineral refining and environmental clean-up. The text examines advances and phenomena observed in ion-exchange systems.

Demonstrating methods for overcoming stability issues in paints, wax dispersions, cosmetics, food products, and other industrial applications, this reference probes theoretical and practical issues surrounding microemulsion science and technology. Featuring the work of 51 international experts and containing almost 1000 instructive tables, equations, and illustrations, this book reviews the performance of, and prospects for, experimental methods such as X-ray diffraction, transmission electron microscopy (TEM), light scattering, small angle neutron scattering, viscosimetry, and nuclear magnetic resonance (NMR) to characterize various aspects of the dispersed phase of microemulsions.

This is one of the first books fully dedicated to the rapidly advancing and expanding research area of deep eutectic solvents. Written by the internationally recognized expert in solution chemistry, it supplies full information regarding preparation of these new eco-friendly solvents, their properties and applications. The current and potential applications of deep eutectic solvents as organic reaction media, catalytic system, in biomass processing, nanotechnology and metal finishing industry, as well as for extraction and separation are extensively discussed.This highly informative and carefully presented book will appeal to practicing chemists (organic chemists, polymer chemists, biochemists) as well as chemical engineers and environmental scientists.

This study focuses on the physical aspects of ultrasonic de-ashing and de-sulfurization, such as cavitation, streaming and their combined effects. Ambedkar Balraj proposes an ultrasound-assisted coal particle breakage mechanism and explores aqueous and solvent-based ultrasonic techniques for de-ashing and de-sulfurization. Ambedkar designs a Taguchi L-27 fractional-factorial matrix to assess the individual effects of key process variables. In this volume he also describes process optimization and scale-up strategies. The author provides a mechanism-based model for ultrasonic reagent-based coal de-sulfurization, proposes a flow diagram for ultrasonic methods of high-throughput coal-wash and discusses the benefits of ultrasonic coal-wash. Coal will continue to be a major fuel source for the foreseeable future and this study helps improve its use by minimising ash and sulfur impurities.

This textbook on fire dynamics provides a comprehensive description of fuels involved in fires, definitions related to fire, thermodynamics for fire calculations, basics of transport processes and fundamental aspects of combustion related to fire, physical descriptions of premixed and non-premixed flames, detailed analysis of the characteristics of fires from solid and liquid fuels, including ignition, spread and burning rates and physical aspects of fire plumes, compartment fires and dust fires. The contents also highlight fundamental aspects related to the evaporation of liquid fuels and pyrolysis of solid fuels which are explained with simplified mathematical expressions. The book includes pedagogical features such as worked examples to illustrate mathematical calculations involved in fire analysis and end-of-chapter review questions. This book proves useful for students, researchers and industry professionals alike.

This thesis focuses on the growth of a new type of two-dimensional (2D) material known as hexagonal boron nitride (h-BN) using chemical vapor deposition (CVD). It also presents several significant breakthroughs in the authors' understanding of the growth mechanism and development of new growth techniques, which are now well known in the field. Of particular importance is the pioneering work showing experimental proof that 2D crystals of h-BN can indeed be hexagonal in shape. This came as a major surprise to many working in the 2D field, as it had been generally assumed that hexagonal-shaped h-BN was impossible due to energy dynamics. Beyond growth, the thesis also reports on synthesis techniques that are geared toward commercial applications. Large-area aligned growth and up to an eightfold reduction in the cost of h-BN production are demonstrated. At present, all other 2D materials generally use h-BN as their dielectric layer and for encapsulation. As such, this thesis lays the cornerstone for using CVD 2D h-BN for this purpose.