Batch Chemical Process Integration: Analysis, Synthesis and Optimization is an excellent source of information on state-of-the-art mathematical and graphical techniques for analysis, synthesis and optimization of batch chemical plants. It covers recent techniques in batch process integration with a particular focus on the capabilities of the mathematical techniques. There is a section on graphical techniques as well as performance comparison between graphical and mathematical techniques. Prior to delving into the intricacies of wastewater minimisation and heat integration in batch processes, the book introduces the reader to the basics of scheduling which is aimed at capturing the essence of time. A chapter on the synthesis of batch plants to highlight the importance of time in design of batch plants is also presented through a real-life case study.

The book is targeted at undergraduates and postgraduate students, researchers in batch process integration, practising engineers and technical managers."

A coherent, concise, and comprehensive course in the statistics needed for a modern career in chemical engineering covers all of the concepts required for the American Fundamentals of Engineering Examination. Statistics for Chemical and Process Engineers (second edition) shows the reader how to develop and test models, design experiments and analyze data in ways easily applicable through readily available software tools like MS Excel (R) and MATLAB (R) and is updated for the most recent versions of both. Generalized methods that can be applied irrespective of the tool at hand are a key feature of the text, and it now contains an introduction to the use of state-space methods. The reader is given a detailed framework for statistical procedures covering: data visualization; probability; linear and nonlinear regression; experimental design (including factorial and fractional factorial designs); and dynamic process identification. Main concepts are illustrated with chemical- and process-engineering-relevant examples that can also serve as the bases for checking any subsequent real implementations. Questions are provided (with solutions available for instructors) to confirm the correct use of numerical techniques, and templates for use in MS Excel and MATLAB are also available for download. With its integrative approach to system identification, regression, and statistical theory, this book provides an excellent means of revision and self-study for chemical and process engineers working in experimental analysis and design in petrochemicals, ceramics, oil and gas, automotive and similar industries, and invaluable instruction to advanced undergraduate and graduate students looking to begin a career in the process industries.

The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; "green" nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namiesnik was a Professor at the Department of Analytical Chemistry, Gdansk University of Technology, Poland. Justyna Plotka-Wasylka is a teacher and researcher at the same department.

This volume discusses the theoretical fundamentals and potential applications of the original electro-Fenton (EF) process and its most innovative and promising versions, all of which are classified as electrochemical advanced oxidation processes. It consists of 15 chapters that review the latest advances and trends, material selection, reaction and reactor modeling and EF scale-up. It particularly focuses on the applications of EF process in the treatment of toxic and persistent organic pollutants in water and soil, showing highly efficient removal for both lab-scale and pre-pilot setups. Indeed, the EF technology is now mature enough to be brought to market, and this collection of contributions from leading experts in the field constitutes a timely milestone for scientists and engineers.

Written by an engineering consultant with over 48 years of experience in the field, this Second Edition provides a reader-friendly and thorough discussion of the fundamental principles and science of cryogenic engineering including the properties of fluids and solids, refrigeration and liquefaction, insulation, instrumentation, natural gas processing, and safety in cryogenic system design.

This collection includes the analysis, development, and operation of high-temperature processes that involve the extraction and processing of material resources, production, and treatment of metals, alloys, and ceramic materials. Contributions describe innovative methods for achieving property enhancement, impurity segregation and removal, byproduct recovery, waste minimization, energy efficiency, and utilization of complex ores. Also included are various technical, economic, and environmental issues associated with commercial-scale high-temperature processing methods.

This book provides practical guidelines to chemical engineers, plant managers, maintenance engineers, and senior managements in modern chemical processing facilities. It provides guidelines to the readers for operational competencies such as hazard identification (HAZID), hazard operability studies (HAZOP), avoiding mistakes in plant facilities to ensure safety, compliance with various statutory rules and regulations; and management of human resources through improved working conditions, provision of safety equipment etc. It further presents technical information on pressure vessels, design of piping and selection of pumping systems, materials for construction and lining of process units operating at high temperature and corrosive conditions, and criteria for selection of different methods for heating of process units. In addition to its application to existing operations, the book includes information on expansion, diversification, and modernization of facilities and guidelines for revival of old and idle plants. Finally, the authors discuss various safety issues, controlling cost of production, and sustainability topics such as planning and implementing co-generation of steam and power, environmental pollution control for chemical plants and safe disposal of hazardous wastes.

Introduction to Sol-Gel Processing introduces undergraduate and graduate students to the field of colloids applied to materials processing, better known as sol-gel processing. It is written for Engineering or Science students in the fields of Chemical Engineering, Materials Processing, Ceramics Engineering, Colloid Science and Mineral Chemistry.
Introduction to Sol-Gel Processing does not intend to be exhaustive on the research done in this field. However the most important facts about the most recent developments, including mixed organic-inorganic sol-gels known as hybrid materials and the use of surfactants and micelles, are addressed. More precisely, the book focuses on gathering the main theories related to sol-gel processing in a comprehensive manner, so as to provide the most important scientific basis to students.
Introduction to Sol-Gel Processing is organized in such a way that each chapter corresponds to one of the main steps in a chronological order of application of sol-gel techniques to the synthesis of materials. The book first presents elementary solvent chemistry, in particular the partial charge model theory. Next, theories on the nucleation and growth of particles and on the steric or electrostatic stabilization (also known as D.L.V.O. theory) of colloidal suspensions, are gathered in a chapter on colloidal particles. Another chapter is devoted to the theories on gelation. Gels, their structure and properties at large such as their swelling, shrinkage or drying behavior, also constitute an important chapter. After drying, gels become almost traditional ceramic materials and they are often submitted to thermal treatments during which they can phase-transform andsinter. Two chapters offer an opportunity to gather the main theories related to these two fields. Finally, the main applications are reviewed according to the domains of application, particularly for coatings, filtering membranes, and catalysts.

The conventional solvents used in chemical, pharmaceutical, biomedical and separation processes represent a great challenge to green chemistry because of their toxicity and flammability. Since the beginning of "the 12 Principles of Green Chemistry" in 1998, a general effort has been made to replace conventional solvents with environmentally benign substitutes. Water has been the most popular choice so far, followed by ionic liquids, surfactant, supercritical fluids, fluorous solvents, liquid polymers, bio-solvents and switchable solvent systems. Green Solvents Volume I and II provides a throughout overview of the different types of solvents and discusses their extensive applications in fields such as extraction, organic synthesis, biocatalytic processes, production of fine chemicals, removal of hydrogen sulphide, biochemical transformations, composite material, energy storage devices and polymers. These volumes are written by leading international experts and cover all possible aspects of green solvents' properties and applications available in today's literature. Green Solvents Volume I and II is an invaluable guide to scientists, R&D industrial specialists, researchers, upper-level undergraduates and graduate students, Ph.D. scholars, college and university professors working in the field of chemistry and biochemistry.

This is a book about mathematical modelling. It focuses on the modelling of the preparation of materials. Materials are important, of course, in an economic sense: the "goods" of goods-and-services are made of materials. This provides a strong incentive to produce good materials and to improve existing materials. Mathematical modelling can help in this regard. Without a doubt, modelling a materials processing operation is not strictly necessary. Materials synthesis and fabrication processes certainly existed before the invention of mathematics and computers, and well before the combined use of mathematics and computers. Modelling can, however, be of assistance--if done properly--and if used properly. The mathematical modelling described in this book is, at its root, a rather formal, structured way of thinking about materials synthesis and fabrication processes. It requires looking at a process as a whole. It requires considering everything that is or might be important. It requires translating the details of a given physical process into one or more mathematical equations. It requires knowing how to simplify the equations without over-simplifying them.

- Microporous Organic Polymers: Design, Synthesis, and Function By J.-X. Jiang and A. I. Cooper - Hydrogen, Methane and Carbon Dioxide Adsorption in Metal-Organic Framework Materials By X. Lin, N. R. Champness, and M. Schroeder -Doping of Metal-Organic Frameworks with Functional Guest Molecules and Nanoparticles By F. Schroeder and R. A. Fischer -Chiral Metal-Organic Porous Materials: Synthetic Strategies and Applications in Chiral Separation and Catalysis By K. Kim, M. Banerjee, M. Yoon, and S. Das -Controlled Polymerization by Incarceration of Monomers in Nanochannels By T. Uemura and S. Kitagawa -Designing Metal-Organic Frameworks for Catalytic Applications L. Ma and W. Lin -Magnetic and Porous Molecule-Based Materials By N. Roques, V. Mugnaini, and J. Veciana

Advances in Catalysis, Volume 71 highlights new advances in the field, with this new volume presenting interesting chapters on a variety of topics, including Advances in the catalytic and photocatalytic behavior of carborane derived metal complexes, Transition metal catalyzed synthesis of derivatives of polyhedral boron hydrides with B-N, B-P, B-O and B-S bonds, Recent advances in transition metal catalyzed selective cage BH functionalization of o-carboranes, Boron Compounds for Catalytic Applications, Regioselective Carborane B-H/C-H Functionalization, and Derivatization of monocarborane and dodecaborate anions by controlled B-H activation.

Catalysis for Enabling Carbon Dioxide Utilization, Volume 70 in the Advances in Catalysis series highlights new advances in the field, with this new volume presenting interesting chapters on a variety of topics, including Catalytic nonreductive CO2 conversions to facilitate fine chemical synthesis, Electrochemical transformation of CO2 into methanol, Electrocatalytic routes towards Carbon Dioxide Activation and Utilization, Visible-light photoredox-catalyzed organic transformations with CO2, Heterogeneous catalysis for the conversion of CO2into cyclic and polymeric carbonates, and Catalytic synthesis of biosourced organic carbonates and sustainable hybrid materials from CO2.

This short monograph focuses on the theoretical backgrounds and practical implementations concerning the thermodynamic modeling of multiphase equilibria of complex reservoir fluids using cubic equations of state. It aims to address the increasing needs of multiphase equilibrium calculations that arise in the compositional modeling of multiphase flow in reservoirs and wellbores. It provides a state-of-the-art coverage on the recent improvements of cubic equations of state. Considering that stability test and flash calculation are two basic tasks involved in any multiphase equilibrium calculations, it elaborates on the rigorous mathematical frameworks dedicated to stability test and flash calculation. A special treatment is given to the new algorithms that are recently developed to perform robust and efficient three-phase equilibrium calculations. This monograph will be of value to graduate students who conduct research in the field of phase behavior, as well as software engineers who work on the development of multiphase equilibrium calculation algorithms.

This book investigates the sustainability performance of system that use microgrids in desalination processes. Climate change may be especially dramatic in its effects on island environments. In these environments, aquifers and wells could become over exploited resulting the use of desalination plans. The synergies between water, energy, and food sectors have been identified as vital in achieving the United Nation's Sustainable Development Goals. The book explores desalination and microgrids technically as well the economic and legal aspects that must be considered in order explore their techno-economic feasibility - analyzing how to improve the desalination process, proposing a method to locate and size a microgrid. Other synergies between the water, energy, and food system are discussed and the benefits to society that might result in these systems. Also, the lessons learned are highlighted in the context of how they may apply to other sustainable enterprises.

This textbook introduces the molecular side of physical chemistry. It offers students and practitioners a new approach to the subject by presenting numerous applications and solved problems that illustrate the concepts introduced for varied and complex technical situations. The book offers a balance between theory, tools, and practical applications. The text aims to be a practical manual for solving engineering problems in industries where processes depend on the chemical composition and physical properties of matter. The book is organized into three main topics: (I) the molecular structure of matter, (II) molecular models in thermodynamics, and (III) transport phenomena and mechanisms. Part I presents methods of analysis of the molecular behavior in a given system, while the following parts use these methods to study the equilibrium states of a material system and to analyze the processes that can take place when the system is in a state of non-equilibrium, in particular the transport phenomena. Molecular Physical Chemistry for Engineering Applications is designed for upper-level undergraduate and graduate courses in physical chemistry for engineers, applied physical chemistry, transport phenomena, colloidal chemistry, and transport/transfer processes. The book will also be a valuable reference guide for engineers, technicians, and scientists working in industry. Offers modeling techniques and tools for solving exercises and practical cases; Provides solutions and conclusions so students can follow results more closely; Step-by-step problem solving enables students to understand how to approach complex issues.

Hybrid composites have exceptional features due to superior mechanical properties, fatigue/impact resistance, and balanced thermal distortion stability. This book covers the latest developments in the hybrid composite materials, processing, characterization, and modeling of materials behaviour. While covering the same, the book also provides insight on its applications in medical science.

This book analyzes hydrocarbon generation and accumulation within space-limited source rocks. The authors draw conclusions based on the principles of basin formation, hydrocarbon generation and accumulation, coupled with the practice of terrigenous basins in eastern China. Hydrocarbon generation and expulsion have been quantitatively assessed in space-limited source rock systems. This book explores new hydrocarbon generation and expulsion models to reflect real geological situations more accurately. The theory and practice proposed in this book challenge the traditional theory of kerogen thermal degradation and hydrocarbon generation.

This book shows the promising future and essential issues on the storage of the supercritical gases, including hydrogen, methane and carbon dioxide, by adsorption with controlling the gas-solid interaction by use of designed nanoporous materials. It explains the reason why the storage of these gases with adsorption is difficult from the fundamentals in terms of gas-solid interaction. It consists of 14 chapters which describe fundamentals, application, key nanoporous materials (nanoporous carbon, metal organic frame works, zeolites) and their storage performance for hydrogen, methane, and carbon dioxide. Thus, this book appeals to a wide readership of the academic and industrial researchers and it can also be used in the classroom for graduate students focusing on clean energy technology, green chemistry, energy conversion and storage, chemical engineering, nanomaterials science and technology, surface and interface science, adsorption science and technology, carbon science and technology, metal organic framework science, zeolite science, nanoporous materials science, nanotechnology, environmental protection, and gas sensors.

Process Control details the core knowledge and practical skills that a successful process control practitioner needs. It explains the essential technologies that are in use in current industrial practice or which may be wanting for the future. The book focuses on practical considerations, not only on those that make a control solution work, but also on those that prevent it from failing, especially for complex control loops and plant-wide control solutions. After discussing the indispensable role of control in modern process industries, the authors concentrate on the skills required for process analysis, control design, and troubleshooting. One of the first books to provide a systematic approach and structured methodology for process analysis and control design, Process Control illustrates that methodology with many practical examples that cover process control, equipment control, and control calculations derived from real projects and applications. The book uses 229 drawings and 83 tables to make the concepts it presents more intuitive and its methodology easy to follow. Process Control will help the practising control engineer to benefit from a wealth of practical experience and good ideas on how to make control work in the real world and students training to take up roles in process control are shown the applied relevance of control theory in the efficient functioning of industrial plant and the considerations needed to make it work. Advances in Industrial Control reports and encourages the transfer of technology in control engineering. The rapid development of control technology has an impact on all areas of the control discipline. The series offers an opportunity for researchers to present an extended exposition of new work in all aspects of industrial control.

This book covers recent advances and future trends in yeast synthetic biology, providing readers with an overview of computational and engineering tools, and giving insight on important applications. Yeasts are one of the most attractive microbial cell factories for the production of a wide range of valuable products, including pharmaceuticals, nutraceuticals, cosmetics, agrochemicals and biofuels. Synthetic biology tools have been developed to improve the metabolic engineering of yeasts in a faster and more reliable manner. Today, these tools are used to make synthetic pathways and rewiring metabolism even more efficient, producing products at high titer, rate, and yield. Split into two parts, the book opens with an introduction to rational metabolic pathway prediction and design using computational tools and their applications for yeast systems and synthetic biology. Then, it focuses on the construction and assembly of standardized biobricks for synthetic pathway engineering in yeasts, yeast cell engineering and whole cell yeast-based biosensors. The second part covers applications of synthetic biology to produce diverse and attractive products by some well-known yeasts. Given its interdisciplinary scope, the book offers a valuable asset for students, researchers and engineers working in biotechnology, applied microbiology, metabolic engineer ing and synthetic biology.

This book is aimed at readers who need to learn the latest solutions for interconnected simulation, testing, and prediction technologies that improve engineering product efficiency, including reliability, safety, quality, durability, maintainability, life-cycle costing and profit. It provides a detailed analysis of technologies now being used in industries such as electronics, automotive, aircraft, aerospace, off-highway, farm machinery, and others. It includes clear examples, charts, and illustrations. This book provides analyses of the simulation, testing, and prediction approaches and methodologies with descriptive, negative trends in their development. The author discusses why many current methods of simulation, testing, and prediction are not successful and describes novel techniques and tools developed for eliminating these problems. This book is a tool for engineers, managers, researches in industry, teachers, and students. Lev Klyatis, Hab. Dr.-Ing., ScD., PhD, Senior Advisor SoHaR, Inc., has been a professor at Moscow State Agricultural Engineering University, research leader and chairman of State Enterprise TESTMASH, and served on the US Technical Advisory Group for the International Electrotechnical Commission (IEC), the ISO/IEC Join Study Group in Safety Aspects of Risk Assessment, the United Nations European Economical Commission, and US-USSR Trade and Economic Council. He is presently a member of World Quality Council, the Elmer A. Sperry Board of Award, SAE International G-41 Reliability Committee, the Integrated Design and Manufacturing Committee and session chairman of SAE International World Congresses in Detroit since 2012. His vast experience and innovation enable him to create a new direction for the successful prediction of product efficiency during any given time, including accurate simulation of real-world conditions, accelerated reliability and durability testing technology, and reducing recalls. His approach has been verified in various industries, primarily automotive, farm machinery, aerospace, and aircraft industries. He has shared his new direction working as the seminar instructor and consultant to Ford, DaimlerChrysler, Nissan, Toyota, Jatko Ltd., Thermo King, Black an Dekker, NASA Research Centers, Karl Schenck, and many others. He holds over 30 patents worldwide and is the author of over 300 publications, including 15 books.

This book uses kinematics, mechanics, mathematics, and so on, to systematically propose the fixturing performance evaluation and fixturing layout planning method. The proposed method is a novel method, including the analysis method of locating determination, the analysis method of workpiece stability, the analysis method of clamping reasonability, the analysis method of workpiece attachment/detachment, the analysis method of locating accuracy, and the planning algorithm of locating point layout, the planning algorithm of clamping force, and so forth. It can enrich and develop the basic theory of computer aided fixture design, change the empirical method of fixture design. The combination of theoretical analysis and mathematical modeling technology can resolve the key problems in the process of fixture design, which will play a certain role in promoting the progress of manufacturing technology, improving the precision and level of product manufacturing, and meeting the higher and higher requirements of mechanical manufacturing industry.

This is the only book that covers containment, specifically for the process industries. This Guide covers the range of containment equipment from simple air-flow control devices to enclosures that restrict exposures to well below a microgram per cubic meter averaged over a working day. The selection of a particular containment system for a particular transfer operation can be difficult because of the wide choice available. This Guide provides a structured approach to the selection process.
Covers the legislation for containment guidelines in the US, UK, and Europe
Provides an exhaustive list of containment equipment, including chapters on maintenance and reliability
Shows the engineer how to develop a containment strategy for his/her plant

This book presents the select proceedings of the National Conference on Research and Developments in Material Processing, Modelling and Characterization (RDMPMC 2020). It covers the recent advances in manufacturing processes. The book explains various manufacturing process technologies based on surface modification, welding, mechanical deformation, and heat treatment. It also covers the topics such as microstructural characterization and properties evaluation, corrosion, and tribology. The book will be useful to researchers, students and professionals working in areas related to materials processing and characterization.