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Books > Professional & Technical > Mechanical engineering & materials > Materials science > Testing of materials > General
Safety of VVER-440 Reactors endeavours to promote an increase in the safety of VVER-440 nuclear reactors via the improvement of fission products limitation systems and the implementation of special non-destructive spectroscopic methods for materials testing. All theoretical and experimental studies performed the by author over the last 25 years have been undertaken with the aim of improving VVER-440 defence in depth, which is one of the most important principle for ensuring safety in nuclear power plants. Safety of VVER-440 Reactors is focused on the barrier system through which the safety principle is organised: * nuclear fuel matrix; * fuel cladding; * integrity of primary circuit; and * confinement system. All these barriers are described in detail and are compared to European standards. Industrial engineers will find Safety of VVER-440 Reactors a useful guide to the safe operation of nuclear power plants and it is an informative source of information for researchers in both industry and academia. Employees of related governmental and regulatory organisations may also benefit from reading this book.
The discovery by J. G. Bednorz and K. A. Mtllier in 1986 that the superconducting state can exist in oxides at temperatures above 30 K stimulated research in the field of superconductivity and opened up a new field of research. Within a few years a large number of cuprate superconductors with transition temperatures well above the boiling point of liquid nitrogen have been found. The possibility of using liquid nitrogen as coolant re-stimulated interest in power applications of supercon ductivity. In this book an overview of the known high-Te superconductors and their physical properties is presented. Aspects related to conductor fabrication and high-current applications are emphasised. The material should be suitable for use in graduate level courses on superconductivity. Researchers in the field may profit from the large number of tables and references describing its status at the end of 1997. An introduction to high-To superconductivity must be based on the fundamental physical principles of normal-state electrical conductivity and the well-known characteristics of conventional superconductors. In Chapter 2 this background is provided. Crystal structures, anisotropic properties and general trends of the critical temperatures of the cuprate superconductors are described in Chapters 3 and 4. The processing of superconductor powders addressed in Chapter 5 affects considerably the current-carrying capacity of high-T. wires. In Chapter 6 several fabrication techniques for superconducting wires are described. In addition, the factors limiting the transport critical currents ofhigh-Te wires are discussed.
3. 1 Techniques of Comminution 35 3. 2 Solid-Solid Reactions 42 3. 2. 1 Mixing and Calcination 42 3. 2. 2 Modem Techniques 45 3. 3 Solution Techniques 46 3. 3. 1 Precipitation and Co-precipitation 46 Forced Hydrolysis 3. 3. 2 49 3. 3. 3 Hydrotbennal Synthesis 51 The Sol-Gel Process 3. 3. 4 53 3. 3. 5 Hydrolysis of Metal-Organics 56 The Emulsion Process 3. 3. 6 56 Solvent Vaporization 3. 4 59 3. 4. 1 Simple Evaporation 59 3. 4. 2 Spray Drying 60 3. 4. 3 Spray Pyrolysis 64 3. 4. 4 Freeze Drying 66 3. 5 Vapour-Phase Techniques 68 3. 5. 1 Vaporization-Condensation 68 3. 5. 2 Vapour-Vapour Reaction 68 3. 5. 3 Vapour-Liquid Reaction 70 3. 5. 4 Vapour-Solid Reaction 71 3. 6 Precursor Decomposition 72 3. 6. 1 Salt Decomposition 72 3. 6. 2 Polymer Pyrolysis 73 4. Synthetic Powders : Options in Preparation 75 4. 0 Introduction 75 4. 1 Single and Multiple Oxide Powders 75 4. 1. 1 Aluminium Oxide 75 4. 1. 2 Zirconium Oxide 85 4. 1. 3 Titanium Oxide 96 4. 1. 4 Magnesium Oxide 99 4. 1. 5 Silicon Dioxide 101 4. 1. 6 Rare Earth Oxides 105 Yttrium Oxide 105 Cerium Oxide 106 4. 1. 7 Zinc Oxide 107 [vi] 4. 1. 8 Mullite 110 4. 1. 9 Magnesium Aluminate Spinel 114 4. 1.
Metal matrix composites are making tangible inroads into the "real" world of engineering. They are used in engineering components such as brake rotors, aircraft parts, combustion engines, and heat sinks for electronic systems. Yet, outside a relatively limited circle of specialists, these materials are mostly unknown. Designers do not as a rule think of using these materials, in part because access to information is difficult as these materials have not really entered engineering handbooks. Metal Matrix Composites in Industry is thus useful to engineers who wish to gain introductory knowledge of these materials and who want to know where "to find" them. Additionally, it provides researchers and academics with a survey of current industrial activity in this area of technology.
Ion implantation offers one of the best examples of a topic that starting from the basic research level has reached the high technology level within the framework of microelectronics. As the major or the unique procedure to selectively dope semiconductor materials for device fabrication, ion implantation takes advantage of the tremendous development of microelectronics and it evolves in a multidisciplinary frame. Physicists, chemists, materials sci entists, processing, device production, device design and ion beam engineers are all involved in this subject. The present monography deals with several aspects of ion implantation. The first chapter covers basic information on the physics of devices together with a brief description of the main trends in the field. The second chapter is devoted to ion im planters, including also high energy apparatus and a description of wafer charging and contaminants. Yield is a quite relevant is sue in the industrial surrounding and must be also discussed in the academic ambient. The slowing down of ions is treated in the third chapter both analytically and by numerical simulation meth ods. Channeling implants are described in some details in view of their relevance at the zero degree implants and of the available industrial parallel beam systems. Damage and its annealing are the key processes in ion implantation. Chapter four and five are dedicated to this extremely important subject.
The NATO Advanced Research Workshop on Fundamental Aspects of Inert Gases in Solids, held at Bonas, France from 16-22 September 1990, was the fifth in a series of meetings that have been held in this topic area since 1979. The Consultants' Meeting in that year at Harwell on Rare Gas Behaviour in Metals and Ionic Solids was followed in 1982 by the Jiilich Inter national Symposium on Fundamental Aspects of Helium in Metals. Two smaller meetings have followed-a CECAM organised workshop on Helium Bubbles in Metals was held at Orsay, France in 1986 while in February 1989, a Topical Symposium on Noble Gases in Metals was held in Las Vegas as part of the large TMS/AIME Spring Meeting. As is well known, the dominating feature of inert gas atoms in most solids is their high heat of solution, leading in most situations to an essentially zero solubility and gas-atom precipita tion. In organising the workshop, one particular aim was to target the researchers in the field of inert-gas/solid interactions from three different areas--namely metals, tritides and nuclear fuels-in order to encourage and foster the cross-fertilisation of approaches and ideas. In these three material classes, the behaviour of inert gases in metals has probably been most studied, partly from technological considerations-the effects of helium production via (n, a) reac tions during neutron irradiation are of importance, particularly in a fusion reactor environ ment-and partly from a more fundamental viewpoint."
Researchers and professionals will find a hands-on guide to successful experiments and applications of modern electroanalytical techniques here. The new edition has been completely revised and extended by a chapter on quartz-crystal microbalances. The book is written for chemists, biochemists, environmental and materials scientists, and physicists. A basic knowledge of chemistry and physics is sufficient for understanding the described methods. Electroanalytical techniques are particularly useful for qualitative and quantitative analysis of chemical, biochemical, and physical systems. Experienced experts provide the necessary theoretical background of electrochemistry and thoroughly describe frequently used measuring techniques. Special attention is given to experimental details and data evaluation.
Within the last 30 years, electron energy-loss spectroscopy (EELS) has become a standard analytical technique used in the transmission electron microscope to extract chemical and structural information down to the atomic level. In two previous editions, Electron Energy-Loss Spectroscopy in the Electron Microscope has become the standard reference guide to the instrumentation, physics and procedures involved, and the kind of results obtainable. Within the last few years, the commercial availability of lens-aberration correctors and electron-beam monochromators has further increased the spatial and energy resolution of EELS. This thoroughly updated and revised Third Edition incorporates these new developments, as well as advances in electron-scattering theory, spectral and image processing, and recent applications in fields such as nanotechnology. The appendices now contain a listing of inelastic mean free paths and a description of more than 20 MATLAB programs for calculating EELS data.
Proceedings of the 3rd Joint International Conference on Hyperfine Interactions and International Symposium on Nuclear Quadrupole Interactions, HFI/NQI 2010 held at CERN, Switzerland, September 13-17, 2010 Reprinted from Hyperfine Interactions Volume. This volume focuses on the most recent studies on all aspects of hyperfine interaction detected by nuclear radiation and nuclear quadrupole interactions detected by resonance methods in the areas of materials, biological and medical science, as well as on contributions on new developments in instrumentation and methods, ab initio calculations and simulations. This volume comprises research papers, reviews, and short communications recording original investigations related to: Theory on Hyperfine Interactions (HFI) and Nuclear Moments; Magnetism and Magnetic Materials (Bulk and Thin Layers); HFI probes in Semiconductors, Metals and Insulators; Lattice Dynamics and Ion-Solid Interactions; Surfaces, Interfaces, Thin Films, and Nano-structures; Resonance Methods; Nuclear Moments, Nuclear Polarization and Spin Dynamics; Investigations in Biology, Chemistry, and Medicine; New Directions and Developments in Methodology. The papers present the latest scientific work of various invited speakers and contributor researchers from the five continents that have brought their perspectives to the meeting.
The clamor for non-carbon dioxide emitting energy production has directly impacted on the development of nuclear energy. As new nuclear plants are built, plans and designs are continually being developed to manage the range of challenging requirement and problems that nuclear plants face especially when managing the greatly increased operating temperatures, irradiation doses and extended design life spans. Materials for Nuclear Plants: From Safe Design to Residual Life Assessments provides a comprehensive treatment of the structural materials for nuclear power plants with emphasis on advanced design concepts. Materials for Nuclear Plants: From Safe Design to Residual Life Assessments approaches structural materials with a systemic approach. Important components and materials currently in use as well as those which can be considered in future designs are detailed, whilst the damage mechanisms responsible for plant ageing are discussed and explained. Methodologies for materials characterization, materials modeling and advanced materials testing will be described including design code considerations and non-destructive evaluation concepts. Including models for simple system dynamic problems and knowledge of current nuclear power plants in operation, Materials for Nuclear Plants: From Safe Design to Residual Life Assessments is ideal for students studying postgraduate courses in Nuclear Engineering. Designers on courses for code development, such as ASME or ISO and nuclear authorities will also find this a useful reference.
A broad range of state-of-the-art methods to determine properties
of clusters are presented. The experimental setup and underlying
physical concepts of these experiments are described.
Kinetic studies have traditionally being extremely useful in characterizing several physical and chemical phenomena in organic, inorganic and metallic systems. It provides valuable qualitative, quantitative and kinetic information on phase transformations, solid state precipitation, crystallization, oxidation and decomposition. Unfortunately, no single reference comprehensively presents nonisothermal kinetic analysis method for the study of complex processes, determining the actual mechanism and kinetic parameters. This book provides a new method for nonisothermal kinetics and its application in heterogeneous solid state processes. In the backdrop of limitations in existing methods, the book presents a brief review of the widely used isothermal and nonisothermal kinetic analysis methods.
This book, "Heat and Mass Transfer in Porous Media," presents a set of new developments in the field of basic and applied research work on the physical and chemical aspects of heat and mass transfer phenomena in a porous medium domain, as well as related material properties and their measurements. The book contents include both theoretical and experimental developments, providing a self-contained major reference that is appealing to both the scientists and the engineers. At the same time, these topics will encounter of a variety of scientific and engineering disciplines, such as chemical, civil, agricultural, mechanical engineering, etc. The book is divided in several chapters that intend to be a short monograph in which the authors summarize the current state of knowledge for benefit of professionals.
In this volume, Prof. Zhang reviews the systematic theoretical studies in his group on the growth mechanisms and properties of silicon quantum dots, nanotubes and nanowires, including: mechanisms of oxide-assisted growth of silicon nanowires, energetic stability of pristine silicon nanowires and nanotubes, thermal stability of hydrogen terminated silicon nanostructures, size-dependent oxidation of hydrogen terminated silicon nanostructures, excited-state relaxation of hydrogen terminated silicon nanodots, and direct-indirect energy band transitions of silicon nanowires and sheets by surface engineering and straining. He also discusses the potential applications of these findings. This book will mainly benefit those members of the scientific and research community working in nanoscience, surface science, nanomaterials and related fields.
Dipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strasso and Anders B. Nielsen.- Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. C. Chan.- Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S. Ulrich.- Probing Quadrupolar Nuclei by Solid-State NMR Spectroscopy: Recent Advances, by Christian Fernandez and Marek Pruski.- Solid State NMR of Porous Materials Zeolites and Related Materials, by Hubert Koller and Mark Weiss.- Solid-State NMR of Inorganic Semiconductors, by James P. Yesinowski.-"
Just over 25 years ago the first laser-excited Raman spectrum of any crystal was obtained. In November 1964, Hobden and Russell reported the Raman spectrum of GaP and later, in June 1965, Russell published the Si spectrum. Then, in July 1965, the forerunner of a series of meetings on light scattering in solids was held in Paris. Laser Raman spectroscopy of semiconductors was at the forefront in new developments at this meeting. Similar meetings were held in 1968 (New York), 1971 (Paris) and 1975 (Campinas). Since then, and apart from the multidisciplinary biennial International Conference on Raman Spectroscopy there has been no special forum for experts in light scattering spectroscopy of semiconductors to meet and discuss latest developments. Meanwhile, technological advances in semiconductor growth have given rise to a veritable renaissance in the field of semiconductor physics. Light scattering spectroscopy has played a crucial role in the advancement of this field, providing valuable information about the electronic, vibrational and structural properties both of the host materials, and of heterogeneous composite structures. On entering a new decade, one in which technological advances in lithography promise to open even broader horirons for semiconductor physics, it seemed to us to be an ideal time to reflect on the achievements of the past decade, to be brought up to date on the current state-of-the-art, and to catch some glimpses of where the field might be headed in the 1990s.
I first learned of the existence of this book on high-temperature superconduc tivity when I received a copy in the office of one of the co-editors, Prof. V. L. Ginzburg, shortly after publication. I had known of the work on problems and prospects of achieving high-temperature superconductors by the members of the I. E. Tamm Department of Theoretical Physics of the P. N. Lebedev Physical Institute. I was naturally anxious to read and study this volume, which inte grates the work of more than a decade. Lest one think that the contributions contained here are of the nature of a reflective looking backward, two important considerations should be kept in mind. First, achievement of high-Tc superconductivity is very much a current and future goal. Elsewhere, one of the authors has described it in these words: "Yes, high-temperature superconductivity is a dream, but a sufficiently realistic one. " Second, the current physics literature contains reports of new and astounding findings-perhaps some of these will later be recognized as precursors to achieving the "dream.
This book provides a profound understanding, which physical processes and mechanisms cause the heat transfer in composite and cellular materials. It shows models for all important classes of composite materials and introduces into the latest advances. In three parts, the book covers Composite Materials (Part A), Porous and Cellular Materials (Part B) and the appearance of a conjoint solid phase and fluid aggregate (Part C).
The Symposium on the Scientific Basis for Nuclear Waste Manage ment was held in the fall of 1979 in Boston, Massachusetts and was one of a number of symposia included in the Annual Meeting of the Materials Research Society. The thrust of this annual Symposium is unique in the area of waste management. Recognizing that this is an area of great complexity which requires contributions from scien tists with many different backgrounds some of which are not normally associated with nuclear energy, the Materials Research Society pro vides a forum for discussions of a wide range of materials behavior and transport phenomena. As can be seen from the list of references in each paper, the authors draw heavily on contributions associated with professional societies in addition to the Materials Research Society, and this annual meeting encourages the cross-fertilization between disciplines that are essential to an adequate treatment of the problems associated with nuclear waste management. The proceed ings of the first Symposium that was held in 1978 was designated as Volume 1 in this series. The third Symposium is scheduled for 1980. The scope of the 1979 Symposium was guided by the Steering Committee: R. L. Schwoebel, Sandia Laboratories, USA (Chairman) W. Carbiener, Battelle Memorial Institute, Columbus, USA D. Ferguson, Oak Ridge National Laboratory, USA W. Heimerl, DWK, Mol, Belgium W. Lutze, Hahn Meitner Institut, Berlin, W. Germany J. D. Mather, Institute of Geological Sciences, Harwell, UK G. Oertel, Department of Energy, USA R.
"Analytic Insights into Intermediate-Energy Hadron-Nucleus Scattering," by R. D. Amado, presents a review of optical diffraction leading into discussions of elastic scattering, single- and multistep inelastic scattering, spin observables, and directions indicated for further research. "Recent Developments in Quasi-Free Nucleon-Nucleon Scattering," by P. Kitching, W. J. McDonald, Th. A. J. Maris, and C. A. Z. Vascon cellos, opens with a comprehensive review of the theory, going on to detail frontier research advances in spin dependence in (p, 2p) scattering, isospin dependence, and other quasi-free reactions. The final chapter, "Energetic Particle Emission in Nuclear Reactions" by D. H. Baal, explores new findings regarding direct interactions in the nucleus, thermalization and multiple scattering in nucleon emission, light fragment formation, and production of intermediate-mass fragments. A valuable and instructive trio of papers, Volume 15 of Advances in Nuclear Physics will be of interest to nonspecialists as well as specialists in the fields of nuclear physics, high-energy physics, and theoretical physics. J. W. NEGELE E. VoGT ix CONTENTS Chapter 1 ANALYTIC INSIGHTS INTO INTERMEDIATE-ENERGY HADRON-NUCLEUS SCATTERING R. D. Amado I. Introduction . . . . . . . . . . . . . . . . . . . . ."
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