This volume contains ?ve chapters. The topics covered are the cathodic reduction of nitrate, for which the key issues are pr- uct selectivity and current ef?ciency; a discussion of ionic l- uids known as molten or fused salts in key industrial processes; the properties of nanowires made of metals and semiconductors by means of electrodeposition into porous templates and template synthesis; and an overview of a range of alloys used in elect- plating, and trends in ammonium electrolysis. Also, included is a review of the applications of synchroton x-ray scattering to the electrochemical interphase. Chapter 1 by Celia Milhano and Derek Pletcher reviews the cathodic reduction of nitrate as a "truly fascinating reaction" since processes for nitrate removal from drinking water and effluents and reducing nitrates in nuclear waste is an essential step in n- lear waste disposal. The authors also review electrochemical membrane technology not involving the cathodic reduction of - trate. In Chapter 2, the authors discuss substances called ionic l- uids, and the fact that this is really a new more modern term for molten or fused salts. However, the label of ionic liquids is usu- ly applied to the liquid state of salts at or near room temperature, which is a way to differentiate low-melting salts from higher me- ing cousins. These molten or fused salts form the basis of several key industrial processes, and this chapter is primarily devoted to the non-haloaluminate ionic liquids as reviewed by Tetsuya Tsuda and Charles L. Hussey.

Strong theoretical and practical knowledge of process control is essential for plant practicing engineers and operators. In addition being able to use control hardware and software appropriately, engineers must be able to select or write computer programs that interface the hardware and software required to run a plant effectively. Designed to help readers understand control software and strategies that mimic human activities, Fundamentals of Automatic Process Control provides an integrated introduction to the hardware and software of automatic control systems.

Featured Topics

• Basic instruments, control systems, and symbolic representations
• Laplacian mathematics for applications in control systems
• Various disturbances and their effects on uncontrolled processes
• Feedback control loops and traditional PID controllers
• Laplacian analysis of control loops
• Tuning methods for PID controllers
• Advanced control systems
• Virtual laboratory software (included on CD-ROM)

Modern plants require operators and engineers to have thorough knowledge of instrumentation hardware as well as good operating skills. This book explores the theoretical analysis of the process dynamics and control via a large number of problems and solutions spread throughout the text. This balanced presentation, coupled with coverage of traditional and advanced systems provides an understanding of industrial realities that prepares readers for the future evolution of industrial operations.

Compiling recent advances in membrane separations technology, this highly relevant book introduces cost-effective solutions for separation problems in a wide range of industries. It discusses membrane use in oil, petrochemicals, and fossil fuels; natural gas exploration; bioseparation; water purification and wastewater treatment; and chemical manufacturing. It describes the role of membrane technologies in resource recovery, pollution prevention, and energy production, as well as environmental monitoring and quality control. A concise resource for emerging technologies, this book provides the tools to implement effective production processes, improve environmental protection and public health, and explore new opportunities for sustainable growth.

The idea of this book is to present the up-to-date research results on Nitrate Esters as explosive materials. It covers many aspects including the material structures, nitrating agent, chemical synthesis devices, preparation technology, and applications etc. In particular, this work sheds light on the comprehensive utilization and thorough destruction of the used Nitrate Easters which is crucial for preventing repeated pollution. This is a highly informative and instructive book providing insight for the researchers working on nitrating theory, energetic materials and chemical equipments.

This immensely practical guide to PIV provides a condensed, yet exhaustive guide to most of the information needed for experiments employing the technique. This second edition has updated chapters on the principles and extra information on microscopic, high-speed and three component measurements as well as a description of advanced evaluation techniques. What's more, the huge increase in the range of possible applications has been taken into account as the chapter describing these applications of the PIV technique has been expanded.

Cleaning Agents and Systems is the first volume in the Handbook for Critical Cleaning, Second Edition.

Should you clean your product during manufacturing? If so, when and how? Cleaning is essential for proper performance, optimal quality, and increased sales. Inadequate cleaning of product elements can lead to catastrophic failure of the entire system and serious hazards to individuals and the general public.

Gain a competitive edge with proven cleaning and contamination-control strategies

A decade after the bestselling original, the Handbook for Critical Cleaning, Second Edition helps manufacturers meet today 's challenges, providing practical information and perspective about cleaning chemistries, equipment, processes, and applications. With 90% new or revised chapters plus supplementary online material, the handbook has grown into two comprehensive volumes: Cleaning Agents and Systems and Applications, Processes, and Controls.

Helping manufacturers become more efficient and productive, these books:

• Show how to increase profitability and meet both existing and expected product demand
• Clarify the sea of print and Internet information about cleaning chemistries and techniques
• Address challenges of performance, miniaturization, and cost, as well as regulatory and supply chain pressures
• Offer clearly written guidance from the viewpoints of more than 70 leading industry contributors in technical, management, academic, and regulatory disciplines

Overview chapters by the editors, industry icons Barbara and Ed Kanegsberg, meld the different viewpoints and compile and critique the options. The result is a complete, cohesive, balanced perspective that helps manufacturers better select, implement, and maintain a quality, value-added cleaning process.

The first volume, Handbook for Critical Cleaning: Cleaning Agents and Systems, gives manufacturers a practical understanding of the variety and functions of cleaning chemistries and cleaning, rinsing, and drying equipment. Topics include aqueous, solvent, and "non-chemical" approaches. Readers can compare process costs, performance, and regulatory issues, and then choose their best option.

Applications, Processes, and Controls is the second volume in the Handbook for Critical Cleaning, Second Edition. Should you clean your product during manufacturing? If so, when and how? Cleaning is essential for proper performance, optimal quality, and increased sales. Inadequate cleaning of product elements can lead to catastrophic failure of the entire system and serious hazards to individuals and the general public. Gain a competitive edge with proven cleaning and contamination-control strategies A decade after the bestselling original, the Handbook for Critical Cleaning, Second Edition helps manufacturers meet today's challenges, providing practical information and perspective about cleaning chemistries, equipment, processes, and applications. With 90% new or revised chapters plus supplementary online material, the handbook has grown into two comprehensive volumes: Cleaning Agents and Systems, and Applications, Processes, and Controls. Helping manufacturers become more efficient and productive, these books: Show how to increase profitability and meet both existing and expected product demand Clarify the sea of print and Internet information about cleaning chemistries and techniques Address challenges of performance, miniaturization, and cost, as well as regulatory and supply chain pressures Offer clearly written guidance from the viewpoints of more than 70 leading industry contributors in technical, management, academic, and regulatory disciplines Overview chapters by the editors, industry icons Barbara and Ed Kanegsberg, meld the different viewpoints and compile and critique the options. The result is a complete, cohesive, balanced perspective that helps manufacturers better select, implement, and maintain a quality, value-added cleaning process. The second volume, Handbook for Critical Cleaning: Applications, Processes, and Controls, addresses how to implement, validate, monitor, and maintain a critical cleaning process. Topics include cleanrooms, materials compatibility, worker safety, sustainability, and environmental constraints. The book shows readers how to draw from diverse disciplines-including aerospace, art conservation, electronics, food, life sciences, military, optics, and semiconductors-to achieve superior productivity.

Recent Developments in Bioenergy Research reviews all these topics, reports recent research findings, and presents potential solutions to challenging issues. The book consolidates the most recent research on the (bio)technologies, concepts and commercial developments that are currently in progress on different types of widely-used biofuels and integrated biorefineries across biochemistry, biotechnology, biochemical engineering and microbiology. Chapters include very recent/emerging topics, such as non-ionic and ionic liquids/surfactants for enhancement of lignocellulose enzymatic hydrolysis and lignocellulose biomass as a rich source of bio-ionic liquids. The book is a useful source of information for those working in the area of- industrial wastewater treatment and microbial fuel cells, but is also a great resource for senior undergraduate and graduate students, researchers, professionals, biochemical engineers and other interested individuals/groups working in the field of biofuel/bioenergy.

New and Future Developments in Microbial Biotechnology and Bioengineering: Recent Advances in Application of Fungi and Fungal Metabolites: Environmental and Industrial Aspects provides a comprehensive overview of recent development and applied aspects of fungi and its metabolites in environmental and industrial settings. Fungi and fungal metabolites have great prospects for developing new products in a wide range of sectors. Many fungal metabolites are environmentally friendly, clean, non-toxic agents used for environmental management practices. This book offers a systems approach and provides a means to share the latest developments and advances about the exploitation of fungal products, including their vide uses in the field of environment and industry.

New and Future Developments in Microbial Biotechnology and Bioengineering: Recent Advances in Application of Fungi and Fungal Metabolites: Biotechnological Interventions and Futuristic Approaches is an invaluable resource for researchers planning to work in applied biotechnological interventions and futuristic approaches to fungi and fungal metabolite utilization. Special emphasis is placed on new research relating to fungal-based recombinant DNA technology and genomics analysis which place yeasts and filamentous fungi at the forefront of various contemporary commercial applications. Written in an easy-to-follow language by active researchers, the book presents cutting-edge fungal biotechnological applications in a manner that is accessible to all.

This book covers different aspects of gas injection, from the classic pressure maintenance operation to enhanced oil recovery (EOR), underground gas storage (UGS), and carbon capture and storage (CCS). The authors detail the unique characteristics and specific criteria of each application, including: material balance equations phase behaviour reservoir engineering well design operating aspects surface facilities environmental issues Examples, data, and simulation codes are provided to enable the reader to gain an in-depth understanding of these applications. Fundamentals and Practical Aspects of Gas Injection will be of use to practising engineers in the fields of reservoir engineering, and enhanced oil recovery. It will also be of interest to researchers, academics, and graduate students working in the field of petroleum engineering.

Shorter reaction times, higher product yields, and enhanced selectivity are some of the advantages microwave heating has over conventional methods, causing its use to transition from a curiosity to mainstream, both in industrial and academic settings. Microwave Heating as a Tool for Sustainable Chemistry showcases the application of microwave heating in a number of areas of preparative chemistry as well as in the biosciences.

From organic chemistry to materials and biological applications

The book begins with an introduction to microwave heating, the physical concepts behind it, its application in synthetic chemistry, and commercially available microwave equipment. It shows how microwave heating can be used to facilitate the clean and sustainable synthesis of organic compounds. The authors examine microwave heating as a tool for sustainable polymer chemistry, with discussions of the use of alternative solvents and feedstocks, the design of degradable polymeric materials, and recycling polymers. They then discuss the significant contribution made by microwave-promoted synthesis in the drug discovery process, with a focus on how the technology has been used to generate discovery chemistry libraries and as a tool for medicinal chemists. Other topics examined in this application-driven text include the use of microwave heating in the preparation of inorganic and organometallic compounds, in the production of inorganic materials, and in the area of biosciences.

Academic and industrial settings

The book examines the scale-up of microwave-promoted chemistry and describes the various approaches and the current commercially available microwave reactors available for scale-up. It also discusses microwave heating as a tool for teaching in the undergraduate organic chemistry laboratory. It explores curriculum, the broad range of reactions that can be performed, and the incorporation of green chemistry principles.

The author maintains a website with supplemental information.

This book describes crucial aspects related to the additive and subtractive manufacturing of different composites. The first half of this book mainly deals with the various types of composite fabrication methods along with the introduction, features and mechanisms and also the processing of composite materials via additive manufacturing route. Also, the thermal, mechanical, physical and chemical properties relevant to the processing of composite materials are included in the chapters. The second half of this book primarily demonstrates an extensive section on the different types of additive manufacturing processes like selective laser sintering, selective laser melting, stereolithography, fused deposition modeling and material jetting used to fabricate the metals and polymers. Also, the chapters address the complete description of fabrication processes for metal matrix composites and polymer matrix composites. Moreover, the different methods adopted such as short peening, micro-machining, heat-treatment and solution treatment to improve the surface improvement are well discussed. This book gives many helps to researchers and students in the fields of the additive and subtractive manufacturing of different composites.

This book investigates in detail the concepts and principles of green chemistry and related methodologies, including green synthesis, green activation methods, green catalysis, green solvents, and green design to achieve process intensification while at the same time ensuring process safety and promoting ecological civilization and environmental protection. Moreover, it incorporates elements of chemical management and chemical education, highlighting chemists' responsibility to protect humankind and foster green and sustainable development in chemistry. Combining Chinese and Belarus wisdom, this book is intended for those working in the chemical industry who are interested in environmental protection and sustainable development, as well as undergraduate and graduate students who are interested in green chemistry and related technologies.

Environmentally Degradable Materials (EDPs) should replace petroleum-based plastics where recycling is not viable for logistic or labor cost reason. This book discusses the general background of obtaining such systems, compatibilization methodologies, control of the rate of degradation and final products after degradation, life time assessment, toxicological aspects, applications and market aspects. This book is a complete guide to the subject of biodegradable materials based on multi-component polymeric systems, mainly such as hydrogels, and interpenetrating polymeric networks. This book is a complete guide to the subject of biodegradable materials based on multicomponent polymeric systems such as mainly hydrogels, interpenetrating polymeric networks.

Smart and Functional Textiles is an application-oriented book covering a wide range of areas from multifunctional nanofinish, wearable e-textiles, textile-based sensors and actuators, thermoregulating textiles, to smart medical textiles and stimuli-responsive textiles. It also includes chapters on 3D printed smart textiles, automotive smart textiles, smart textiles in military and defense, as well as functional textiles used in care and diagnosis of Covid-19.

Waste minimisation has a number of aims which include enhancing the intrinsic selectivity of any given process, providing a means of recovering reagents in a form which allows easy regeneration and the replacement of stoichiometric processes with catalytic ones. Solids, as catalysts or as supports for other reagents, offer potential for benefit in all these areas. This monograph provides an overview of the properties of the more useful solid catalysts and supported reagents, and highlights their most valuable applications in the preparation of organic chemicals in liquid phase reactions. Clean Synthesis Using Porous Inorganic Solid Catalysts and Supported Reagents is concerned with the use of solid catalysts in the clean synthesis of organic chemicals. The emphasis is on chemical processes of importance to the manufacture/preparation of fine and speciality chemicals, chemical intermediates and pharmaceutical intermediates, especially where catalysis is not currently used or where current catalysts are homogeneous, leading to difficult separation procedures and unacceptable levels of waste. This book focuses on solid catalysts based on inorganic supports and covers the emerging area of chemically modified mesoporous solid catalysts.

Analytical Methods for Biomass Characterization and Conversion is a thorough resource for researchers, students and professors who investigate the use of biomass for fuels, chemicals and products. Advanced analytical chemistry methods and techniques can now provide detailed compositional and chemical measurements of biomass, biomass conversion process streams, intermediates and products. This volume from the Emerging Issues in Analytical Chemistry series brings together the current knowledge on each of these methods, including spectroscopic methods (Fourier Transform Infrared Spectroscopy, Near-infrared Spectroscopy, Solid State Nuclear Magnetic Resonance), pyrolysis (Gas Chromatography/Mass Spectrometry), Liquid Chromatography/High Performance Liquid Chromatography, Liquid Chromatography/Mass Spectrometry, and so on. Authors David C. Dayton and Thomas D. Foust show how these can be used for measuring biomass composition and for determining the composition of intermediates with regard to subsequent processing for biofuels, bio-chemicals and bio-based products.

Surface and colloid chemistry principles impact many aspects of our daily lives, ranging from the cleaners and cosmetics we use to combustion engines and cement. Exploring the range of this field of study, Surface and Colloid Chemistry provides a detailed analysis of its principles and applications and demonstrates how they relate to natural phenomena and industrial processes.

Surface and colloid chemistry at work in nature and industry:

• rain drops
• combustion engines
• soap bubbles
• foam
• food products
• air pollution
• waste-water treatment
• washing and cleaning
• cosmetics
• painting and printing
• oil and gas production
• oil spills
• plastics and polymers
• biology and pharmaceuticals
• milk products
• cement
• adhesive
• coal

The book begins with an introduction to surfaces and colloids. It describes basic considerations regarding liquids and capillarity, and examines the liquid-solid interface phenomena. It explores the physicochemical properties of surfactants, Langmuir-Blodgett films, adsorption on solid surfaces, and adsorption as it relates to cleaning processes. Then the author examines colloidal systems and thin liquid films before moving on to emulsion science and technology. The final chapter provides examples of applications in science and a range of industries.

Examples and Illustrations

Integrating real-world examples throughout the text, this volume stimulates readers to consider both fundamental theory and industrial applications. More than 100 figures elucidate the concepts described in the text. Sample questions and answers are provided where appropriate, along with detailed data and discussions. Pertinent references are offered to facilitate further study.

The purpose of this volume is to provide a brief review of the previous work on model reduction and identifi cation of distributed parameter systems (DPS), and develop new spatio-temporal models and their relevant identifi cation approaches.

In this book, a systematic overview and classifi cation on the modeling of DPS is presented fi rst, which includes model reduction, parameter estimation and system identifi cation. Next, a class of block-oriented nonlinear systems in traditional lumped parameter systems (LPS) is extended to DPS, which results in the spatio-temporal Wiener and Hammerstein systems and their identifi cation methods. Then, the traditional Volterra model is extended to DPS, which results in the spatio-temporal Volterra model and its identification algorithm. All these methods are based on linear time/space separation. Sometimes, the nonlinear time/space separation can play a better role in modeling of very complex processes.

Thus, a nonlinear time/space separation based neural modeling is also presented for a class of DPS with more complicated dynamics. Finally, all these modeling approaches are successfully applied to industrial thermal processes, including a catalytic rod, a packed-bed reactor and a snap curing oven. The work is presented giving a unifi ed view from time/space separation. The book also illustrates applications to thermal processes in the electronics packaging and chemical industry. This volume assumes a basic knowledge about distributed parameter systems, system modeling and identifi cation. It is intended for researchers, graduate students and engineers interested in distributed parameter systems, nonlinear systems, and process modeling and control.

This edited book explores the use of surfactants in upstream exploration and production (E&P). It provides a molecular, mechanistic and application-based approach to the topic, utilising contributions from the leading researchers in the field of organic surfactant chemistry and surfactant chemistry for upstream E&P. The book covers a wide range of problems in enhanced oil recovery and surfactant chemistry which have a large importance in drilling, fracking, hydrate inhibition and conformance. It begins by discussing the fundamentals of surfactants and their synthesis. It then moves on to present their applicability to a variety of situations such as gas injections, shale swelling inhibition, and acid stimulation. This book presents research in an evolving field, making it interesting to academics, postgraduate students, and experts within the field of oil and gas.

This book presents experimental and numerical methods that have been developed during six years of targeted research within the DFG priority program SPP 1740, elucidating the interaction between hydrodynamics, mass transfer and transport as well as chemical reactions in bubbly flows. A special feature of this book is its focus on an interdisciplinary research approach with contributions from chemistry, mathematics and engineering sciences, providing enhanced or novel experimental methods, models and numerical simulations. This book provides fundamental knowledge to students about the current state of knowledge regarding transport processes in reactive bubbly flows as well as to scientists, emphasizing pressing research questions and further current demands for fundamental research. Engineers from the chemical industries will get valuable insights into relevant gas-liquid processes and benefit from recommendations concerning the design of gas-liquid reactors and laboratory experiments for studying the performance of gas-liquid reactions in their own lab.

Although computer technology has dramatically improved the analysis of complex transport phenomena, the methodology has yet to be effectively integrated into engineering curricula. The huge volume of literature associated with the wide variety of transport processes cannot be appreciated or mastered without using innovative tools to allow comprehension and study of these processes. Connecting basic principles with numerical methodology for solving the conservations laws, Computational Transport Phenomena for Engineering Analyses presents the topic in terms of modern engineering analysis. The book includes a production quality computer source code for expediting and illustrating analyses of mass, momentum, and energy transport.

The text covers transport phenomena with examples that extend from basic empirical analyses to complete numerical analyses. It includes a computational transport phenomena (CTP) code written in Fortran and developed and owned by the authors. The code does not require a lease and can run on a PC or a supercomputer. The authors also supply the source code, allowing users to modify the code to serve their particular needs, once they are familiar with the code. Using the CTP code, grid generation and solution procedures are described and visual solution presentations are illustrated thus offering extensive coverage of the methodology for a wide range of applications.

The authors illustrate and emphasize that the very general solutions afforded by solving the unsteady, multidimensional transport equations for real multicomponent fluids describe an immense body of physical processes. Bringing together a wealth of professional and instructional experience, this book stresses a problem-solving approach that uses one set of computational and graphical tools to describe all aspects of the analysis. It provides understanding of the principles involved so that code improvements and/or use of commercial codes can be accomplished knowledgeably.

In the development of next-generation nanoscale devices, higher speed and lower power operation is the name of the game. Increasing reliance on mobile computers, mobile phone, and other electronic devices demands a greater degree of speed and power. As chemical mechanical planarization (CMP) progressively becomes perceived less as black art and more as a cutting-edge technology, it is emerging as the technology for achieving higher performance devices. Nanoparticle Engineering for Chemical-Mechanical Planarization explains the physicochemical properties of nanoparticles according to each step in the CMP process, including dielectric CMP, shallow trend isolation CMP, metal CMP, poly isolation CMP, and noble metal CMP. The authors provide a detailed guide to nanoparticle engineering of novel CMP slurry for next-generation nanoscale devices below the 60nm design rule. They present design techniques using polymeric additives to improve CMP performance. The final chapter focuses on novel CMP slurry for the application to memory devices beyond 50nm technology. Most books published on CMP focus on the polishing process, equipment, and cleaning. Even though some of these books may touch on CMP slurries, the methods they cover are confined to conventional slurries and none cover them with the detail required for the development of next-generation devices. With its coverage of fundamental concepts and novel technologies, this book delivers expert insight into CMP for all current and next-generation systems.

This book introduces the fundamentals and principles of laser shock peening (LSP) for aeronautical materials. It focuses on the innovation in both theory and method related to LSP-induced gradient structures in titanium alloys and Ni-based alloys which have been commonly used in aircraft industries. The main contents of the book include: the characteristics of laser shock wave, the formation mechanism of gradient structures and the strengthening-toughing mechanism by gradient structures. The research has accumulated a large amount of experimental data, which has proven the significant effectiveness of LSP on the improvement of the fatigue performance of metal parts, and related findings have been successfully applied in aerospace field. This book could be used by the researchers who work in the field of LSP, mechanical strength, machine manufacturing and surface engineering, as well as who major in laser shock wave and materials science.