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Books > Professional & Technical > Industrial chemistry & manufacturing technologies > Industrial chemistry > General
Because enzyme-catalyzed reactions exhibit higher enantioselectivity, regioselectivity, substrate specificity, and stability, they require mild conditions to react while prompting higher reaction efficiency and product yields. Biocatalysis in the Pharmaceutical and Biotechnology Industries examines the use of catalysts to produce fine chemicals and chiral intermediates in a variety of pharmaceutical, agrochemical, and other biotechnological applications. Written by internationally recognized scientists in biocatalysis, the authors analyze the synthesis of chiral intermediates for over 60 brand-name pharmaceuticals for a wide range of drug therapies and treatments. From starting material to product, the chapters offer detailed mechanisms that show chiral intermediates and other by-products for each reaction-including hydrolytic, acylation, halogenation, esterification, dehalogenation, oxidation-reduction, oxygenation, hydroxylation, deamination, transamination, and C-C, C-N, C-O bonds formation. Cutting-edge topics include advanced methodologies for gene shuffling and directed evolution of biocatalysts; the custom engineering of enzymes; the use of microbial cells and isolated biocatalysts; the use of renewable starting materials; and generating novel molecules by combinatorial biocatalysis and high-throughput screening. Focusing on industrial applications, the book also considers factors such as bulk processes, instrumentation, solvent selection, and techniques for catalyst immobilization, reusability, and yield optimization throughout. Biocatalysis in the Pharmaceutical and Biotechnology Industries showcases the practical advantages and methodologies for using biocatalysts to develop and produce chiral pharmaceuticals and fine chemicals.
The phenomenon known as fluorescence is now widely used in the chemical and life sciences largely due to the development of highly sophisticated fluorescent probe chemistries and the commercial availability of these probes as well as the development of novel microscopy approaches. Introduction to Fluorescence helps readers acquire a sound understanding of basic fluorescence theory and practice. It describes general principles in a straightforward way and uses examples from a variety of disciplines to demonstrate them. In color throughout, the book takes readers through the history of important discoveries to the most current advances. It introduces the fundamentals of the fluorescence phenomenon and gives detailed examples of fluorescence applications in the molecular life sciences, including biochemistry, biophysics, clinical chemistry and diagnostics, pharmaceutical science, and cell and molecular biology. The author presents the basic theories underlying the applications and offers in-depth information on practical aspects. Along with a list of references in each chapter, the text incorporates more than 250 figures that clearly illustrate the concepts and gives the chemical structures of the most widely used fluorescent molecules. In addition, the appendix provides a "Rogue's Gallery" of the most common errors and pitfalls to avoid.
Silicone is an important class of materials used in applications that range from industrial assembly to everyday consumer products. Silicones are often delivered and synthesized in dispersion forms, the most common being liquid-in-liquid (emulsion), solid-in-liquid (suspension), air-in-liquid (foam) and solid-in air (powder). This book compiles a carefully selected number of topics that are essential to the understanding, creative design and production of silicone dispersions. As such, it provides the first unified description of silicone dispersions in the literature.
To meet changing market demands that have stringent emission standards and to ensure proper performance in refinery units, evaluation of novel catalyst designs and results from material characterization and testing of catalysts are of crucial importance for refiners as well as for catalyst manufacturers. This book highlights recent developments in the application of refinery catalysts in selected units such as fluid catalytic cracking (FCC), hydrogen production for hydroprocessing units, hydrotreating, hydrocracking, and sustainable processing of biomass into biofuels.
Drying of solids is one of the most common, complex, and energy-intensive industrial processes. Conventional dryers offer limited opportunities to increase energy efficiency. Heat pump dryers are more energy and cost effective, as they can recycle drying thermal energy and reduce CO2, particulate, and VOC emissions due to drying. This book provides an introduction to the technology and current best practices and aims to increase the successful industrial implementation of heat pump- assisted dryers. It enables the reader to engage confidently with the technology and provides a wealth of information on theories, current practices, and future directions of the technology. It emphasizes several new design concepts and operating and control strategies, which can be applied to improve the economic and environmental efficiency of the drying process. It answers questions about risks, advantages vs. disadvantages, and impediments and offers solutions to current problems. Discusses heat pump technology in general and its present and future challenges. Describes interesting and promising innovations in drying food, agricultural, and wood products with various heat pump technologies. Treats several technical aspects, from modeling and simulation of drying processes to industrial applications. Emphasizes new design concepts and operating and control strategies to improve the efficiency of the drying process.
Traditionally, design and control decisions are made in sequential stages over the life cycle of a chemical plant. In the design phase, the optimal operating conditions and the corresponding material and energy balance data are established mainly on the basis of economic considerations. In the subsequent step, the control systems are configured to maintain the key process conditions at the fixed nominal values. Because it is often desirable to address the operability issues at the earliest possible stage before stipulation of control schemes, the systematic incorporation of flexibility analysis in process synthesis and design has received considerable attention in recent years. This book focuses to a large extent on computation and implementation methods of deterministic performance measures, i.e., the steady-state, volumetric, dynamic and temporal flexibility indices, in various applications. The formal definitions of several available performance indices, their mathematical formulations, and the corresponding algorithms and codes are provided in sufficient detail to facilitate implementation. To show the utility of flexibility analyses, the book presents several practical case studies including membrane modules and heat-exchanger networks, solar-driven membrane distillation desalination systems, and hybrid power generation systems. It also includes MATLAB and GAMS codes.
Encapsulation is a topic of interest across a wide range of scientific and industrial areas, from pharmaceutics to food and agriculture, for the protection and controlled release of various substances during transportation, storage, and consumption. Since encapsulated materials can be protected from external conditions, encapsulation enhances their stability and maintains their viability. This book offers a comprehensive review of conventional and modern methods for encapsulation. It covers various thermal and nonthermal encapsulation methods applied across a number of industries, including freeze drying, spray drying, spray chilling and spray cooling, electrospinning/electrospraying, osmotic dehydration, extrusion, air-suspension coating, pan coating, and vacuum drying. The book presents basic fundamentals, principles, and applications of each method, enabling the reader to gain extended knowledge. The choice of the most suitable encapsulation technique is based on the raw materials, the required size, and the desirable characteristics of the final products.
Answering the need for information that could revolutionize the development of alternate solar energy sources and the reduction of atmospheric contaminants, Semiconductor Photochemistry and Photophysics reflects renewed interest inspired by the unique properties of nanocrystalline semiconductor particles. It provides a thorough overview and describes fundamental research aimed at understanding the underlying mechanisms of the cells and looks at the application of nanocrystalline TiO2 as a photocatalyst for environmental remediation. Key topics include semiconductor photoelectrochemistry, dye-sensitized solar cells, and photocatalytic treatment of chemical waste.
Elastomer Technology Handbook is a major new reference on the science and technology of engineered elastomers. This contributed volume features some of the latest work by international experts in polymer science and rubber technology. Topics covered include theoretical and practical information on characterizing rubbers, designing engineering elastomers for consumer and engineering applications, properties testing, chemical and physical property characterization, polymerization chemistry, rubber processing and fabrication methods, and rheological characterization. The book also highlights both conventional and emerging market applications for synthetic rubber products and emphasizes the latest technology advancements. Elastomer Technology Handbook is a "must have" book for polymer researchers and engineers. It will also benefit anyone involved in the handling, manufacturing, processing, and designing of synthetic rubbers.
This book is designed to provide authoritative reviews in the field of modern electroanalytical chemistry defined in its broadest sense. It is helpful to practicing analytical chemists interested in learning about and applying electroanalytical techniques.
This book presents the most up-to-date information on a wide range of developments in chromatographic methods and applications. It provides timely, cutting-edge reviews in the fields of bio-, analytical, organic, polymer, and pharmaceutical chemistry.
Chemical Analysis provides non invasive and micro-analytical techniques for the investigation of cultural heritage materials. The tools and techniques, discussed by experts in the field, are of universal, sensitive and multi-component nature.
The presence of cationic pollutant metals in municipal wastewater effluent is a concern because stringent discharge requirements cannot always be met with conventional treatment methods. Attempts to improve metal removal are often unsuccessful because a significant fraction of the cationic metals are complexed by the synthetic chelating agent ethylenediamine tetraacetic acid (EDTA). To identify practical approaches for improving metal removal, an analytical method for measuring metal-EDTA complexes was used to survey metal speciation at a series of wastewater treatment plants. Following these analyses, bench-scale experiments were conducted. The survey data indicated that pollutant metal-EDTA complexes account for a significant fraction of the dissolved metals in wastewater. The bench-scale studies indicated that ferric chloride addition improves the removal of copper and zinc by approximately 20%. To test the results of the bench-scale experiments, a full-scale experiment was conducted by interrupting chemical addition at a municipal wastewater treatment plant that normally adds ferric chloride during primary treatment. Results indicated that ferric chloride addition had a slight impact on metal speciation but no effect on metals removal. The lack of an effect was attributed to changes in metal speciation that occurred during primary treatment irrespective of ferric chloride addition.
The study of environmental interfaces and environmental catalysis is central to finding more effective solutions to air pollution and in understanding of how pollution impacts the natural environment. Encompassing concepts, techniques, and methods, Environmental Catalysis provides a mix of theory, computation, analysis, and synthesis to support the latest applications in biocatalysis, green chemistry, environmental remediation and our understanding of the interaction of pollutants with natural systems. The book focuses on several aspects of environmental catalysis. Surface catalysis of airborne particles - including ice, trace atmospheric gases, aerosolized soot nanoparticles, and mineral dust surfaces - as well as particles in contact with ground water and their role in surface adsorption, surface catalysis, hydrolysis, dissolution, precipitation, oxidation and ozone decomposition is explored. It continues by presenting catalysis as the key technology for treating emissions and reducing waste by-products. The authors review the theory behind catalytic converters and discuss the effectiveness of several catalysts, including zeolites and nanoparticles, in treating emissions, aromatic hydrocarbons, and chemical warfare agents. They also survey the use of biocatalysis in environmental remediation, and industrial processes, particularly in the production of transportation fuels, fine chemicals, and pharmaceuticals. Then the authors explain how enzymes can remove chlorinated organics and metals and how microbes can metabolize toxic chemicals from groundwater. Lastly, they discuss the principles of green chemistry, including the use of environmentally benign solvents, biphasic catalysts, and other alternative solvents to recover and recycle catalysts based on heavy metals. With increasing ground water pollution, increasing particulates in the atmosphere, and the increasing need to remove pollutants from industrial and automotive sources, Environmental Catal
Written for anyone who is considering implementing or currently using TPM or looking for ways of improving their current process, the second edition focuses on the financial approach to the subject-a methodology that produces quantifiable results allowing a TPM program to be sustainable. Completely revised and updated, this classic reference is the most flexible and comprehensive approach documented to date. Additionally, it offers a significant amount of new material, such as: 1. Various case studies that show how to explain the value of OEE to everyone in the organization from the senior executive to the shop floor personnel. 2. OEE discussions showing how to dollarize results and present the financial terms to executive financial personnel. 3. A clarification of the goals and objectives of TPM, allowing TPM Champions to clearly present a TPM business case to their organizations.4. The pitfalls that may be encountered during TPM implementation and how to avoid or correct these problems.
Considers groundbreaking developments in cosmeceuticals and the two-in-one shampoo! Multifunctional Cosmetics examines the execution details one should consider when creating multifunctional products shows how to design tests to support claims considers the role of packaging in multifunctional products explores products designed to deliver, enhance, or prolong color as they clean and condition hair analyzes the growing importance of shower gels and bath products that perform multiple functions such as cleansing, conditioning, and coloring demonstrates how antiperspirants/deodorants use dually functional formulas to control body odor indicates how to introduce moisturizing or conditioning properties into products that have a different primary function Complemented by more than 300 references, figures, and tables, Multifunctional Cosmetics is an excellent resource for pharmaceutical formulation, cosmetic, and fragrance chemists, scientists, and technologists; cosmetics, pharmaceutical, chemical, and biochemical engineers; skin physiologists and biologists; pharmacists and pharmacologists; dermatologists; quality control and assurance managers; and regulatory personnel; and upper-level undergraduate and graduate students in these disciplines.
This excellent book systematically identifies the issues surrounding the effective linking of project management techniques and engineering applications. It is not a technical manual, nor is it procedure--led. Instead, it encourages creative learning of project engineering methodology that can be applied and modified in different situations. In short, it offers a distillation of practical 'on--the job' experience to help project engineers perform more effectively. While this book specifically addresses process plants, the principles are applicable to other types of engineering project where multidisciplinary engineering skills are required, such as power plant and general factory construction. It focuses on the technical aspects, which typically influence the configuration of the plant as a whole, on the interface between the various disciplines involved, and the way in which work is done -- the issues central to the co--ordination of the overall engineering effort. It develops an awareness of relationships with other parties -- clients, suppliers, package contractors, and construction managers -- and of how the structure and management of these relationships impact directly on the performance of the project engineer. Readers will welcome the author's straightforward approach in tackling sensitive issues head on. COMPLETE CONTENTS* Introduction* A process plant* A project and its management* A brief overview* The engineering work and its management* The project's industrial environment* The commercial environment* The contracting environment* The economic environment* Studies and proposals* Plant layout and modelling* Value engineering and plant optimization* Hazards, loss, and safety* Specification, selection and purchase* Fluid transport* Bulk solids transport* Slurries and two--phase transport* Hydraulic design and plant drainage* Observations on multidiscipline engineering* Detail design and drafting* The organization of work* Construction* Construction contracts* Commissioning* Communication* Change and chaos* Fast--track projects* Advanced information management* Project strategy development* Key issues summary
At the interface of chemical industry operations, equipment
manufacturer input, and the scientific literature, Industrial
Crystallization of Melts explores and explains melt crystallization
and purification in the industrial arena. This comprehensive
account details the orderly conversion of melts into solid, salable
end materials and procedures for purification by remelting;
summarizes key theoretical concepts relating to crystalline matter
and instationary heat transfer; and surveys the equipment available
for specific processes. It also offers over 100 tested equations,
as well as clear-cut methods for handling organic melts that call
for special crystallization provisions.
This Special Issue titled "Recent Advances in Sensing Technology" in the book series of "Lecture Notes in Electrical Engineering" contains the extended version of the papers selected from those that were presented at the 3rd International Conference on Sensing Technology (ICST 2008) which was held in November 30 to December 3, 2008 at National Cheng-Kung University, Tainan, Taiwan. A total of 131 papers were presented at ICST 2008, of which 19 papers have been selected for this special issue. This Special Issue has focussed on the recent advancements of the different aspects of sensing technology, i.e. information processing, adaptability, recalibration, data fusion, validation, high reliability and integration of novel and high performance sensors. The advancements are in the areas of magnetic, ultrasonic, vision and image sensing, wireless sensors and network, microfluidic, tactile, gyro, flow, surface acoustic wave, humidity, gas, MEMS thermal and ultra-wide band. While future interest in this field is ensured by the constant supply of emerging modalities, techniques and engineering solutions, many of the basic concepts and strategies have already matured and now offer opportunities to build upon.
The Eighth International Conference on Miniaturized Systems in Chemistry and Life Science - MicroTas 2004 - is an annual meeting focusing on the research, development and application of miniaturized technologies and methodologies in chemistry and life science. The conference is celebrating its tenth anniversary after the first workshop at the University of Twente, The Netherlands in 1994. This research field is rapidly developing and changing towards a domain where core competence areas such as microfluidics, micro- and nanotechnology, materials science, chemistry, biology, and medicine are melting together to a truly interdisciplinary meeting place. This volume is the first in a two volume set, a valuable reference collection to all working in this field.
The Eighth International Conference on Miniaturized Systems in Chemistry and Life Science - MicroTas 2004 - is an annual meeting focusing on the research, development and application of miniaturized technologies and methodologies in chemistry and life science. The conference is celebrating its tenth anniversary after the first workshop at the University of Twente, The Netherlands in 1994. This research field is rapidly developing and changing towards a domain where core competence areas such as microfluidics, micro- and nanotechnology, materials science, chemistry, biology, and medicine are melting together to a truly interdisciplinary meeting place. This volume is the second in a two volume set, a valuable reference collection to all working in this field.
Thermal enrichment of coldwater streams by heated stormwater in summer months is often overlooked and even exacerbated by traditional management practices that typically account for flow moderation and pollutant removal only. Initiated in 1999, this study evaluated and identified innovative and traditional approaches to moderate this temperature impact by monitoring and analyzing the hydrologic and thermal regimes of an urban stormwater treatment system consisting of two traditional wet detention ponds and an enhanced natural wetland. Data analysis clearly shows temperature increases in the open detention ponds and the ability of the wetland to mitigate this thermal enrichment. Event-based thermal loading and temperature regime analysis indicated flow reduction via infiltration and effective vegetative cover in the wetland were the primary mechanisms for mitigating stormwater thermal enrichment. Using the concept of temperature equivalent, we also established the locations and strength of thermal enrichment areas. A heat transfer model was developed to simulate runoff temperature. Results indicated that rainfall characteristics, temperature difference between rainfall and the ground surface, and the runoff flow depth were the most important factors affecting runoff temperature.
The batch distillation process has existed for many centuries. It is perhaps the oldest technology for separating or purifying liquid mixtures and is the most frequently used separation method in batch processes. In the last 25 years, with continuous development of faster computers and sophisticated numerical methods, there have been many published works using detailed mathematical models with rigorous physical property calculations and advanced optimisation techniques to address several important issues, such as selection of column configurations, design, operation, off-cut recycling, use of batch distillation in reactive and extractive modes, etc. Batch Distillation: Design and Operation presents excellent, important contributions of many researchers from around the globe, including those of the author and his co-workers.
Pressure-Sensitive Adhesives and Applications, Second Edition explains how pressure-sensitive adhesives (PSAs) work, why they are used, and the technology used to manufacture them. This second edition features the latest developments in the field. Dr. Benedek discusses the factors that affect the rheology and special flow characteristics responsible for the adhesivity of liquid and solid PSAs. His book explores the viscoelastic behavior of PSAs, and compares them to plastics, rubbers, and polymers properties and examines the parameters that influence the conversion process of PSAs from the coating of carrier materials to the properties of the final laminate. The author covers adhesion/cohesion balance, time-temperature dependence of pressure sensitivity, chemical composition, coating properties, and coating processes affect the adhesive properties of PSA and their end products and how application-specific performance indices are used to determine the formulation and manufacture of raw materials. In addition, up-to-date coating machines, converting technology, and environmental considerations in the manufacture of PSA final products as well as industry-specific methods of testing for quality assurance and control are discussed. Pressure-Sensitive Adhesives and Applications, Second Edition combines the theoretical basis of pressure sensitivity with the practical aspects of manufacturing, testing, and use of PSAs. Readers are offered an exhaustive as well as comparative look at the engineering of plastics, adhesives, and pressure-sensitives, resulting in an indispensable, up-to-date reference for adhesive and polymer chemists and technologists.
This expert volume provides specialized coverage of the current state of the art in carbon gels. Carbon gels represent a promising class of materials with high added value applications and many assets, like the ability to accurately tailor their structure, porosity, and surface composition and easily dope them with numerous species. The ability to obtain them in custom shapes, such as powder, beads, monoliths, or impregnated scaffolds opens the way towards numerous applications, including catalysis, adsorption, and electrochemical energy storage, among others. Nevertheless, it remains a crucial question as to which design synthesis and manufacturing processes are viable from an economic and environmental point of view. The book represents the perspectives of renowned specialists in the field, specially invited to conduct a one-day workshop devoted to carbon gels as part of the 19th International Sol-Gel Conference, SOL-GEL 2017, held on September 3rd, 2017 in Liege, Belgium. Addressing properties and synthesis through applications and industry outlook, this book represents essential reading for advanced graduate students through practicing researchers interested in these exciting materials. |
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